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Result of the Month (ROM) April 2025

Influence of hydrogen-bonded 3-mercaptopropionic acid bilayers on binary self-assembled monolayer formation

ROM

Accelerating Materials Innovation 

Electron Spectroscopy

Photoelectron Spectroscopy | © Scienta Omicron

Scanning Probe Microscopy

LT STM Lab | © Scienta Omicron

Thin Film Deposition

Lab10 MBE System | © Scienta Omicron

Result of the Month (ROM), April 2025

Influence of hydrogen-bonded 3-mercaptopropionic acid layers on binary self-assembled monolayer formation

The influence of the monolayer order, defect density, and bilayer formation on the formation of binary self-assembled monolayers (SAMs) was investigated via the solution-phase displacement of 3-mercaptopropionic acid (MPA) by 1-decanethiol (DT). The ultrahigh vacuum scanning tunnelling microscopy results confirm that well-ordered, pristine MPA SAMs are displaced at slower rates than MPA SAMs with less long-range order and greater defect density. Furthermore, MPA samples containing regions of an MPA bilayer displayed the slowest rates of displacement with DT. For pristine MPA samples and MPA samples with regions of an MPA bilayer, displacement with DT resulted in the formation of the low-density, lying down phase of DT. Our results suggest that the presence of an MPA bilayer, the result of hydrogen bonding between carboxylic acid groups in MPA, significantly lowers the rate of total displacement of MPA by DT compared to moderately defected MPA SAMs. These results highlight the importance of the structure, composition, and intermolecular forces, such as hydrogen bonding, when considering binary SAM formation via solution-phase displacement methods.

Latest news

Introducing ARCTIC SPM Lab

We are excited to officially announce the launch of ARCTIC, our latest ultra-high vacuum (UHV) scanning probe microscopy (SPM) platform, designed for cutting-edge research at the intersection of nanoscience and quantum technology.

The ARCTIC SPM represents our latest innovation in modular, ultra-low-temperature scanning probe microscopy. Built on our newly developed ARCTIC closed-cycle cooling platform, it combines cutting-edge technology with user-friendly operation.

With the ARCTIC SPM LAB, you benefit from unattended, continuous cooling, eliminating the complexities of handling extreme temperatures. This system ensures virtually unlimited measurement time while delivering the stability traditionally associated with liquid helium cryostat-based SPMs.

Designed for maximum flexibility, the ARCTIC SPM features a unique horizontal cooling power feed, resulting in a compact footprint. Its open-access design allows for unrestricted entry from all sides, empowering your experiments with unmatched versatility.

News PEAK-1.5 Now Available for Download!

We're thrilled to announce that PEAK-1.5 is now ready for download at the Scienta Omicron Customer Portal. Here's a quick overview of the new features you can expect with this release:

  • New Sequence Control for easier setup of measurements
  • A fresh Sequence View with Spectrum Region Summaries for better control during measurement
  • Introduction of Continuous Pass Energies for optimisation of instrument resolution and data recording efficiency (requires a new software license)
  • Introduction of a Detector Overexposure Monitor to protect the MCP/CMOS detector from intensity overload

Sample Manipulators

Open and Closed Cycle Sample Manipulators

When aiming at high experimental energy resolution for ARPES measurement, it is crucial to achieve ultra-low sample temperatures to quench thermal broadening. This is possible with state-of-the-art cryo manipulators reaching sample temperatures from < 3.5 K and featuring up to 6 fully motorized axes for a large range of movements. The manipulators are available as open and closed cycle. Open cycle manipulators reach lower temperature specifications and are rapidly cooled down from room temperature to 10 K in 15 min. The low He consumption below 1 l/h at ultimate temperature and the possibility to operate with liquid nitrogen at higher temperatures ensure a low operating cost. Closed cycle manipulators have no He consumption providing unlimited holding time.

Service Upgrade

PEAK Slit Control

Optimal analyser settings with remote control

In photoelectron spectroscopy measurements, there is always a trade-off between signal intensity and resolution. Optimising this balance is the key to obtaining smooth and sharp spectra within the shortest time possible. For hemispherical analysers, this trade-off is controlled by the selected entrance slit and pass energy.
PEAK Slit Control replaces manual slit changes at the analyser with a motorised and software-controlled slit. With the control of all analyser settings, easy and quick optimisation of signal intensity versus resolution is possible.

About Us 

Scienta Omicron is a leading innovator in Surface Science and Nanotechnology. At our technology centres in Uppsala, Sweden and Taunusstein, Germany we develop and produce high-tech instruments. Our instruments support top researchers globally and are serviced by our four regional hubs in USA, China, Japan and Germany.

We provide state of the art instruments in Electron Spectroscopy, Scanning Probe Microscopy and Thin Film Deposition. Focusing on the race for new unique materials and solutions, in areas like – smarter batteries, next generation electronics, quantum technologies, solar energy, intelligent sensors and advanced materials, Scienta Omicron enables development of tomorrow´s materials.

THE SCIENTA GROUP: One Group, Two Leading Brands

Since 1983 the combined companies, including Scienta Omicron and Scienta Envinet (former Scienta Sensor Systems and Envinet GmbH respectively) that make up the Scienta Scientific Group have been leading the development of ultra high vacuum research and analysis equipment in the fields of Surface Science, Material Physics, UHV technology and Radiation Detection, resulting in scientific breakthroughs, Nobel Prizes and outstanding industrial equipment.